SINGLE OIL SOAP EXPERIMENT: PHASE 3 - One Year Later

I can't believe it's already been a year since I started the SINGLE OIL SOAP EXPERIMENT. My 30 lovely  bars (well, one not so lovely) have been patiently awaiting their day in the spotlight since I last critiqued them at 8 weeks into cure. Well, 9+ months later, they have not failed to deliver some interesting results!

A refresher on the experiment for those new to the blog:
I took 15 common soaping oils and made a soap with 170 grams of each single oil and a 41% lye solution. They were each cut in two, with one labeled "A" and one labeled "B". "A" soaps were stored in a cardboard box in a dry location. "B" soaps were stored in a cardboard box in a damp location. They were weighed, pH tested, and lather-tested upon unmolding, and then again at 8 weeks, and comparisons were noted. Phase 3 is their current states of being at one year old. I have not re-weighed them today, but did lather tests and inspected for rancidity and finger-test hardness (not specifically solubility). My method for lather testing* was to run the bar under warm water for 10 seconds, roll between my hands with light friction for 10 seconds, take the picture, rinse, and dry my hands between each soap. I do have a reverse-osmosis water softener so results in hard water may (and most likely will) differ. I'm also disclosing which oils I personally use, so that you can determine for yourself whether I'm objective enough for your discriminating taste. I feel I was pretty objective, because, let's face it...at 40 years old, I can't remember which number stood for what oil at a year later until looking at my notes to write this post...

* Friction helps produce more bubbles and thicker lather with any soap - and these soaps are no exception. Check out Olive Oil's lather with more friction added. Makes a big difference! But for the purposes of this experiment, and to keep a "controlled" study (as controlled as I can be in my kitchen!), I wanted preliminary results that someone with no experience with handmade soap would get.

And so without further adieu...

1. TALLOW

Tallow - One Year Old

Tallow - Lather - One Year Old

Tallow is still a hard, white bar, very close to it's original size and shape with no signs of DOS ("Dreaded Orange Spots" - the soapmaker's term for rancidity). Not much lather to speak of, with very fine bubbles. Not very conditioning on the hands, but not drying. In my humble opinion, though I do not personally use Tallow (or any animal fats), it seems to be a good oil for bulk - a filler oil, if you will.

2. RICE BRAN

Rice Bran - One Year Old

Rice Bran - Lather - One Year Old

Rice Bran had thin light bubbles and felt good one the skin. The bars were hard and free of DOS. Would be a nice substitute for Olive Oil.

3. OLIVE (Castille)

Olive - One Year Old

Olive - Lather at Unmolding, 8 weeks, & One Year

If I used a lot of friction, this is the lather produced by One Year Old Castille

Castille Soap, or 100% Olive Oil Soap, has been lauded as the most gentle and hardest bar of soap you can make...and while that may be true, if you're looking for a nice bubbly bar - this isn't it. Though not as slimy of a lather as it was in its infancy, it still was more of a lotion-type feel, which is great if that's what you're going for. I didn't find it any more "moisturizing" or skin-softening than Rice Bran or Avocado. I wanted to finally be blown away by it's gentleness and get why everyone flips their wigs over Castille soap, but alas...
I use Olive Oil in 90% of my soaps however, and adore it blended with other oils that bring the other properties I'm looking for.
A very hard bar without a spot of DOS. Very much as it was, though harder and not as slimy.

4. LARD

Lard - One Year Old

Lard - DOS spot on bottom left corner of "A" soap (Dry location)

Lard - Lather - One Year Old

I was surprised to find a spot of DOS on the "A" Lard soap from the dry location. Otherwise, Lard didn't change much - a lotion type lather with no bubbles. Once again, I feel it may be good as a bulk or "filler" oil, like Tallow or Palm. Lard Soapers rave over it's conditioning properties, so if you're open to using an animal fat, it may be worth a shot when formulated with other oils.

5. SAFFLOWER

Safflower - One Year Old - DOS on bottom left corner of "B"

Safflower - One Year Old - The beginnings of DOS on back of "A" & "B"

Safflower - Lather - One Year

Safflower is probably not one of the more common soaping oils, but there is use for it out there. At one year, it's beginning to show DOS on the backs of both "A" and "B" soaps. It is hard, but not super hard with very scant, almost imperceptible lather.

6. SOYBEAN

Soybean did not blow me away, though I'm suprised to say that there is no DOS at one year on either "A" or "B" soap. Not a super hard bar - I can't completely dent it, but there is a bit of "give" when pressing hard with my thumb. A little bit of lather, but in general, nothing to get excited about.

7. AVOCADO

Avocado - One Year Old

Avocado - DOS spot on lower right back side of "B" soap

Avocado - Lather - One Year

I do personally use Avocado oil in a few of my soaps, mostly replacing part (or all) of the Olive Oil. However, on it's own? Well, it was starting a spot of DOS on the back of the "B" soap. About the same hardness as Soybean, and about the same type of lather. It does feel very nice on the skin though - soft and smooth with no drag. I definitely recommend it as a percentage of the formula, though maybe not as a stand alone oil.

8. PALM

Palm - One Year

Palm - Lather - One Year

I'm an Organic Sustainable Palm Oil user (Soaper's Choice), and this test has reinforced why I continue to use Palm Oil. Please don't read that as I don't care about environmental or animal issues in favor of making soap - I most certainly do care about both issues! I also realize that the Palm Oil issue is much bigger and more complex than to just stop using it. Everything is connected and every action creates a reaction. But that topic is for another post (that I will hopefully get to this summer).
Back on topic...the Palm soap is free of DOS, super hard, with a thick creamy lather. While I don't find it the most moisturizing of oils, my skin felt soft without the drag that it had after using the Palm soap in the beginning of this experiment. And while I compared Palm to Tallow and Lard as bulkers or fillers, I feel that Palm brings a bit more to the table than either of the other two.

9. CORN

The Corn oil soap surprised me...I expected a bit of DOS, but it was spotless and very much like it was at the beginning of the experiment. A pretty hard bar with a moderate lather of thin fluffy bubbles.It wasn't a stand out on any front, but I would consider it more than I would have before this experiment.

10. SUNFLOWER

Sunflower - One Year Old...and obvious DOS on "A"

Sunflower - DOS on backs of "A" & "B"

Sunflower - Lather - One Year

And here's where things start to get ugly. And slimy. But mostly really ugly. DOS city, man. Not really stinky, but a bit of that "old oil" smell" - you would think it would smell worse by the way it looks. And strangely enough, the dry location "A" soap is worse (covered all over in orange-ness) than the wet location "B" soap (orange-ness on back only). It's a shame too, because the lather definitely improved since the beginning of the experiment - it actually had nice foamy bubbles!. It is soft, tacky, and starting to get a bit slimy. I would highly suggest checking out the High Oleic Sunflower Oil, as it supposedly has a longer shelf life, though I can not attest to that myself.

11. GRAPESEED

Grapeseed - One Year Old

Grapeseed - Progression of DOS

Grapeseed - Lather - One Year

And things get even uglier. And slimier. And smellier. And just gross. But no surprises here, really. We could see that Grapeseed was a mess from the beginning. It took forever to unmold because it was so soft. At eight weeks, it was already a soft, yellowy mess and smelled rancid. At one year, things have just progressed to the point of no return. There was actually a bit of wet, orange slime under this soap in the box. And the lather was actually orange! Ugh.
Funny thing: the other day I was reading an article from a business that shall remain nameless, stating that the main oil used in many of their products (salves, mainly) was Grapeseed, because of it's "long shelf life".
Wh-what?! 
Way before this experiment, years ago, I had hands-on experience with Grapeseed Oil going rancid pretty darn quickly - less than 3 months in a product made for myself. Thank goodness I didn't sell it...that would have killed my chances of a soap empire. And this is why I do not use Grapeseed Oil in any of my products. Even with an anti-oxidant, you would still need a good preservative to make this last long-term. For a personal use product at home that will be used within a week or so, it may be fine.

I HAVE AN OBSERVATION: The Sunflower soap was next to the Grapeseed soap (in numerical order) in the box. At the 8 week mark, I separated them to opposite corners to see whether the DOS could spread from one soap to another. Now, I'm no scientist, per se. and this wasn't a sterile lab environment with controls (other than those mentioned above)...but I think it's possible that DOS can spread from one soap to another if they touch.

12. CANOLA

Another surprise here with the nice clean white bar - no DOS, pretty hard bar with decent light lather. Nothing to write home about, but a possible cheap alternative for experimenters out there.

13. COCONUT

Coconut - One Year with a small DOS on "B" soap

Coconut - Lather - One Year

Coconut always delivers on lather - that's no surprise. The dot of DOS on the side of the "B" bar is. I've never, ever had DOS on a soap made with Coconut Oil. Which brings me back to the question made in the observation above: Can one DOS infected soap contaminate another otherwise DOS-free soap? Hmm...I think I need to do another experiment...
Super hard white bar, thick bubbly lather...and I don't find it as drying as some other people do (even though my skin is dry by nature). It's still my Number One Oil, despite that random DOS dot. I think it's a fluke. In general, Coconut Oil, when stored properly, can last up to 2 years or more.

14. PEANUT

Peanut - One Year Old with small DOS on front lower right of "B"

Peanut - One Year Old - possible DOS on  back of "A"

Peanut - Lather - One Year

Peanut was a good bubbler right out of the gate. A nice hard bar with good lather, but it did get a spot of DOS on the front of "B", and what I think will eventually be DOS on the back of "A" (I don't think it's just discoloration). A good cheap-ish alternative for the experimenters.

15. CASTOR

Castor - One Year Old

Castor - Lather - One Year Old

Castor is the one oil I use in all of my soaps, usually between 5 - 8%. I find it adds nice moisturizing properties. Castor is always recommended to add bubbly lather (by me, too), even though you wouldn't think so from this picture. It's not a stand alone oil, though washing my hands with this one last left them soft and supple - no waxy drag that I noticed at the beginning of the experiment. Super hard bar, no DOS.

I wanted to add a few pictures for reference:
This is a soap I was gifted by another soapmaker and it is 2 years old.
Their recipe consisted of Lard, Crisco, Coconut, and Olive Oils (and I believe was scented with Cinnamon essential oil). The discoloration on the corner was there when I opened it, so I doubt it's DOS and may just be discolored from oxidation of the essential oil (my guess):

Fellow Soaper's 2 Year Old Soap

Fellow Soaper's 2 Year Old Soap

Fellow Soaper's Lather after 2 years

This is a piece of soap from the same soaper, discolored more from DOS (the same batch as the previous photos). It is very dry and hard, with a pretty strong rancid odor: Stored in a perforated ziploc bag in the linen closet in the bathroom.

Fellow Soaper's Non-DOS soap, and DOS infected soap from same batch - 2 years old

And here is a 1+ year old bar from a batch I made for my older son called Black Winter Sky. It's formula was Olive, Coconut, Palm, and Castor, scented with Clove, Patchouli, and Cedarwood essential oils, and colored with Woad (it was more blue, but faded to grey) and swirled (ITP) with Activated Charcoal. No DOS and was stored unwrapped in the linen closet in the bathroom.
The same lather test was done on both my soap and the fellow soaper's that I used in this experiment.

Black Winter Sky

So did you learn anything new from this experiment?
Did it get your gears spinning on a new oil to use?
Did it reinforce what you already use?
I can't wait to hear your deductions, observations, and opinions!